The sodium and barium isothiocyanate complexes of 6,7,9,10,12,13,20,21,23,24,26,27-dodecahydro-dibenzo[b,n]-1,4,7,10,13,16,19,22-octaoxacyclotetracosin (dibenzo-24-crown-8 ether=DB24C8) were synthesized and analyzed by X-ray diffraction.
The sodium complex, [Na(DB24C8)(NCS)(H2O)] 1, crystallizes in the orthorhombic space group Fdd2 with 16 molecules in the unit cell...
Keywords: Dibenzo-24-crown-8 ether, Na, Ba complexes, Single crystal structure analysis, X-ray diffraction
03/2006 | Zeitschrift für Kristallographie, Oldenbourg Wissenschaftsverlag