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R. Steininger, Werner Freyland

SAXS Spectrometer for High Temperature Studies of Fluids

A new construction of a high temperature set-up for small angle X-ray scattering (SAXS) measurements on corrosive and volatile fluid systems is presented. The sample cell from single crystal sapphire is sealed with a special metal wire technique. The cell with the surrounding high temperature furnace is integrated in a homemade SAXS-spectrometer. This technique has been employed up to 1000°C for the example of SAXS-measurements on fluid K_xKCl_1-x solutions which are briefly discussed.

Zeitschrift für Physikalische Chemie, Oldenbourg Wissenschaftsverlag

Print ISSN: 0942-9352
Volume: 214, 05/2000
Pages: 541

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