27-s 263Db was produced in the 249Bk ( 18O, 4n) reaction at 93MeV. The activity was transported by a He/KCl-jet to the laboratory where it was collected for 15min and then subjected to a chemical separation specific for group-4 elements. The activity was dissolved in 0.5M unbuffered α-HiB and eluted from a cation-exchange column. The effluent was made 9M in HCl and group-4 tetrachlorides were extracted into TBP/Cyclohexane which was evaporated to dryness on a Ta disc. The Ta discs were assayed for α and SF activity. A SF activity with a half life on the order of 20min was observed and assigned to the nuclide 263Rf. It is formed by electron-capture decay of 263Db with a decay branch of 3+4-1.
Print ISSN: 0033-8230
Volume: 91, 01/2003
Pages: 059